A BRIEF COURSE IN QUALITATIVE CHEMICAL ANALYSIS

By H. DATIL

CONTENTS 1 MICELLE ENHANCED FLUORIMETRIC AND THIN LAYER CHROMATOGRAPHY DENSITOMETRIC METHODS FOR THE DETERMINATION OF (±) CITALOPRAM AND ITS S – ENANTIOMER ESCITALOPRAM 2 A MULTIDISCIPLINARY INVESTIGATION TO DETERMINE THE STRUCTURE AND SOURCE OF DIMERIC IMPURITIES IN AMG 517 DRUG SUBSTANCE 3 SELECTIVE SPECTROPHOTOMETRIC AND SPECTROFLUOROMETRIC METHODS FOR THE DETERMINATION OF AMANTADINE HYDROCHLORIDE IN CAPSULES AND PLASMA VIA DERIVATIZATION WITH 1,2-NAPHTHOQUINONE-4-SULPHONATE 4 ANALYTICAL APPLICATIONS OF REACTIONS OF IRON(III) AND HEXACYANOFERRATE(III) WITH 2,10-DISUBSTITUTED PHENOTHIAZINES 5 QUANTITATIVE MASS SPECTROMETRIC ANALYSIS OF ROPIVACAINE AND BUPIVACAINE IN AUTHENTIC, PHARMACEUTICAL AND SPIKED HUMAN PLASMA WITHOUT CHROMATOGRAPHIC SEPARATION 6 KINETIC SPECTROPHOTOMETRIC DETERMINATION OF CERTAIN CEPHALOSPORINS IN PHARMACEUTICAL FORMULATIONS 7 UNDERSTANDING STRUCTURAL FEATURES OF MICROBIAL LIPASES— AN OVERVIEW 8 SIGNIFICANCE ANALYSIS OF MICROARRAY FOR RELATIVE QUANTITATION OF LC/MS DATA IN PROTEOMICS 9 DETERMINATION OF KEY INTERMEDIATES IN CHOLESTEROL AND BILE ACID BIOSYNTHESIS BY STABLE ISOTOPE DILUTION MASS SPECTROMETRY 10 A DYNAMIC PROGRAMMING APPROACH FOR THE ALIGNMENT OF SIGNAL PEAKS IN MULTIPLE GAS CHROMATOGRAPHY-MASS SPECTROMETRY EXPERIMENTS 11 SOLID-PHASE EXTRACTION AND REVERSE-PHASE HPLC: APPLICATION TO STUDY THE URINARY EXCRETION PATTERN OF BENZOPHENONE-3 AND ITS METABOLITE 2,4-DIHYDROXYBENZOPHENONE IN HUMAN URINE 12 A SIMPLE AND SELECTIVE SPECTROPHOTOMETRIC METHOD FOR THE DETERMINATION OF TRACE GOLD IN REAL, ENVIRONMENTAL, BIOLOGICAL, GEOLOGICAL AND SOIL SAMPLES USING BIS(SALICYLALDEHYDE) ORTHOPHENYLENEDIAMINE 13 PALM-BASED STANDARD REFERENCE MATERIALS FOR IODINE VALUE AND SLIP MELTING POINT 14 BIOMEDICAL AND FORENSIC APPLICATIONS OF COMBINED CATALYTIC HYDROGENATION-STABLE ISOTOPE RATIO ANALYSIS 15 IDENTIFICATION AND QUANTITATION OF ASPARAGINE AND CITRULLINE USING HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) 16 SEARCHING FOR NEW CLUES ABOUT THE MOLECULAR CAUSE OF ENDOMYOCARDIAL FIBROSIS BY WAY OF IN SILICO PROTEOMICS AND ANALYTICAL CHEMISTRY 17 EVALUATION OF FRUCTOOLIGOSACCHARIDES AND INULINS AS POTENTIALLY HEALTH BENEFITING FOOD INGREDIENTS BY HPAEC-PED AND MALDI-TOF MS 18 PREPARATION, CHARACTERIZATION, AND ANALYTICAL APPLICATION OF RAMIPRIL MEMBRANE-BASED ION-SELECTIVE ELECTRODE 19 GC-MS STUDIES OF THE CHEMICAL COMPOSITION OF TWO INEDIBLE MUSHROOMS OF THE GENUS AGARICUS 20 STRUCTURAL ANALYSIS OF THREE NOVEL TRISACCHARIDES ISOLATED FROM THE FERMENTED BEVERAGE OF PLANT EXTRACTS